Oxygen Demand (BOD) P,G Cool, 4 C 1000 ml 48 hours Boron P HNO3,pH<2 100 ml 6 months Chemical Oxygen Demand (COD) P,G H2SO4,pH<2,Cool,4 C 100 ml 28 days Chloride P,G None required 100 ml 28 days Chlorine Residual P,G Cool, 4 C; protect from light 500 ml 2 hours Color P,G None required 500 ml ASAP